Mechanical Behavior of Transparent Spinel Fabricated by Spark Plasma Sintering
نویسندگان
چکیده
In this work, a transparent nanostructured ceramic magnesium aluminate spinel (MgAl2O4) was fabricated by Spark Plasma Sintering (SPS) from commercial nano-powders at different temperatures (1300, 1350 and 1400 °C). The sintered samples were thoroughly examined to assess their microstructural, optical, mechanical properties. Various techniques such as SEM, AFM, spectrophotometer with an integrating sphere, instrumented Vickers indenter, Pin-on-Disk tribometer, scratch tester, sandblasting device employed characterize the samples. results indicated significant impact of sintering temperature on properties Particularly, T = °C exhibited highest Real In-line Transmission (RIT 72% 550 nm 80% 1000 nm). These demonstrated hardness value (HV 16.7 GPa) compared those 1300 15.6 15.1 GPa). measured fracture toughness increased substantially increasing temperature. Similarly, tribological study revealed that friction coefficient temperature, lowest wear rate. Additionally, tests confirmed influence spinels. Overall, presented best compromise in terms all evaluated
منابع مشابه
In-situ Fabrication of Transparent Magnesium Aluminate Spinel by Spark Plasma Sintering
Transparent polycrystalline spinel ceramic was fabricated without any sintering aids by spark plasma sintering method of a mixture of Al2O3 and MgO powders for only 10min soak at 1250°C. Densification, microstructure and optical transparency of spinel were examined. The spinel exhibits an in-line transmission of 55% for a visible-wavelength of 470nm and high hardness value of 2040 HV.
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ژورنال
عنوان ژورنال: Ceramics
سال: 2023
ISSN: ['2571-6131']
DOI: https://doi.org/10.3390/ceramics6020072